The 1H and 13C NMR resonances for a novel distamycin conjugate, 3-[1-methyl-4-[1-methyl-4-[1-methyl-4-[N1-[5-methyl-2,4(1H,3H)pyrimidinedione]acetylamino]pyrrole-2-carboxamido]pyrrole-2-carboxamido]pyrrole-2-carboxamido]propionamidine hydrochloride, were assigned, using the concerted application of one- and two-dimensional NMR techniques including nuclear Overhauser effect difference, DEPT, HMQC and HMBC expts.
Synthesis and spectral study of a novel distamycin conjugate
BARALDI, Pier Giovanni;ROMAGNOLI, Romeo;
2003
Abstract
The 1H and 13C NMR resonances for a novel distamycin conjugate, 3-[1-methyl-4-[1-methyl-4-[1-methyl-4-[N1-[5-methyl-2,4(1H,3H)pyrimidinedione]acetylamino]pyrrole-2-carboxamido]pyrrole-2-carboxamido]pyrrole-2-carboxamido]propionamidine hydrochloride, were assigned, using the concerted application of one- and two-dimensional NMR techniques including nuclear Overhauser effect difference, DEPT, HMQC and HMBC expts.File in questo prodotto:
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