5-(Pyrrolidin-2-yl)tetrazole functionalized silica prepared by photoinduced thiol-ene coupling is packed into a short stainless steel column. The resulting packed-bed microreactor is conveniently heated to perform environmentally benign continuous-flow aldol reactions with good stereoselectivities, complete conversion efficiencies, and long term stability of the packing material
Silica-supported 5-(pyrrolidin-2-yl)tetrazole: development of organocatalytic processes from batch to continuous-flow conditions
MASSI, Alessandro;BORTOLINI, Olga;CAVAZZINI, Alberto;PASTI, Luisa;COSTA, Valentina;GRECO, Roberto;CACIOLLI, Lorenzo
2012
Abstract
5-(Pyrrolidin-2-yl)tetrazole functionalized silica prepared by photoinduced thiol-ene coupling is packed into a short stainless steel column. The resulting packed-bed microreactor is conveniently heated to perform environmentally benign continuous-flow aldol reactions with good stereoselectivities, complete conversion efficiencies, and long term stability of the packing materialFile in questo prodotto:
Non ci sono file associati a questo prodotto.
I documenti in SFERA sono protetti da copyright e tutti i diritti sono riservati, salvo diversa indicazione.
