The ESIMS technique, combined with 1H NMR evidence, provides a precise inventory of the catalytic TiIV precursors and the characterization of the reactive peroxometal complex involved in enantioselective sulfoxidation employing the TiIV–homochiral trialkanolamine–alkylhydroperoxide system.
Use of electrospray ionization mass spectrometry to characterize chiral reactive intermediates in a titanium alkoxide mediated sulfoxidation reaction
BORTOLINI, Olga;
1997
Abstract
The ESIMS technique, combined with 1H NMR evidence, provides a precise inventory of the catalytic TiIV precursors and the characterization of the reactive peroxometal complex involved in enantioselective sulfoxidation employing the TiIV–homochiral trialkanolamine–alkylhydroperoxide system.File in questo prodotto:
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